File Entry: GLIBENCLAMIDE Complexes ( Complexes of Mg,Cr,Ni,Zn and Cd salts )Synthesis and characterization

Created: 2012-07-24 11:33:50      Last updated: 2012-07-24 11:33:51
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Version created on: 2012-07-24 11:33:50


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The N-acetyl derivative of β-phenethylamine is reacted with chlorosulfonic acid to form the para sulfonyl chloride derivative. This is then subjected to ammonolysis, followed by base-catalyzed removal of the acetamide. This is then acylated with 2-methoxy-5-chlorobenzoic acid chloride to give the amide intermediate. This is then reacted with cyclohexyl isocyanate to yield the sulfonylurea glibenclamide


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